Synthesis of Triazole derivative: [4-(benzylideneamino)-5-phenyl -4H-1,2,4 – triazole-3-thiol]

Authors

  • Ashok Kumar Singh Department of Chemistry, Tri-Chandra Multiple Campus, Tribhuvan University
  • Khem Raj Kandel Department of Chemistry, Tri-Chandra Multiple Campus, Tribhuvan University

DOI:

https://doi.org/10.3126/jncs.v30i0.9391

Keywords:

Triazole derivative, Schiff base, 4-(benzylideneamino)-5-phenyl -4H-1, 2, 4 – triazole-3-thiol

Abstract

The basic nucleus 4-(amino)-5-phenyl-l-4H-1,2,4-triazole-3-thiol has been synthesized by cyclisation of potassium dithiocarbazinate with hydrazine hydrate using water as solvent under reflux condition for 3-4 h. The compound which has been synthesized successfully was subjected to condensation with benzaldehyde to synthesize 4-(benzylideneamino)-5-phenyl -4H-1,2,4 – triazole-3-thiol (Schiff base). The compounds were confirmed by physical parameters (melting point), chromatographic methods (TLC) and spectroscopic methods (IR and NMR).

DOI: http://dx.doi.org/10.3126/jncs.v30i0.9391

Journal of Nepal Chemical Society

Vol. 30, 2012

Page:  174-177

Uploaded date: 12/20/2013

 

 

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Published

2013-12-19

How to Cite

Singh, A. K., & Kandel, K. R. (2013). Synthesis of Triazole derivative: [4-(benzylideneamino)-5-phenyl -4H-1,2,4 – triazole-3-thiol]. Journal of Nepal Chemical Society, 30, 174–177. https://doi.org/10.3126/jncs.v30i0.9391

Issue

Vol. 30 (2012)

Section

Articles

License

© Journal of Nepal Chemical Society